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Download Advances in Biomedical Engineering. Volume 4 by J.H.U. Brown, J.F. Dickson PDF

By J.H.U. Brown, J.F. Dickson

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Since the source does not contain a filament, air or vaporized organic solvents m a y be drawn through t h e reaction chamber without damage to or malfunction of the source. Under these conditions t h e instrument will detect organic compounds (and some inorganic compounds like a m monia and carbon monoxide) with low ionization potential in extremely low concentration. Since organic solvents do not injure t h e source, and m a y serve as a source of r e a c t a n t ions, it m a y be possible t o devise a liquid c h r o m a t o g r a p h - m a s s spectrometer-computer assembly analogous to G C - M S - C O M systems.

HORNING, AND R. Ν. STILLWELL High-resolution mass spectrometry is usually carried out with p h o t o plate recording or by scanning methods. If a photoplate is used, t h e operation is off-line of necessity, but optical comparators are now generally used with on-line or virtual on-line computer acquisition of d a t a . A small computer system can be used in on-line fashion with a highresolution mass spectrometer (resolution about 1:10,000) ; an example of a suitable system is t h a t described by Klimowski et al.

Helium is generally used as a carrier gas, and the initial flow is reduced to about 2 ml per minute entering the source. At t h e time of development of this separator, very little was known about methods for concentrating a solute in t h e gas phase, and the solution to the problem was an i m p o r t a n t contribution in t h e development of gas-phase analytical methodology. T h e R y h a g e separator, while based on the differential diffusion of carrier gas and solute, involves high-speed projection of the gas stream through a low-pressure region.

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